Nine plates of DIN EN 10025-2 S275JR steel (base metal) were machined, each one with 6.35 × 130 × 330 mm. A square groove was machined in the center of each plate to simulate a standardized bevel joint, onto which weld beads were subsequently deposited using AWS ER70S-6 filler metal. The welds are shown in Fig. 1. The mechanical properties and chemical composition of the base material are presented in Table 1.
The GMAW process was employed to weld the nine samples using a Yaskawa MH6 welding robot, a Yaskawa DX100 controller, and a Fronius TransPuls Synergic welding source. The equipment is shown in Fig. 2. AWS ER70S-6 welding wire with a diameter of 1 mm was employed. The only adjustable welding parameter was the flow rate of the shielding gas, which was modified at three different levels (Table 2).
Table 1
– Mechanical properties and chemical composition of DIN EN 10025-2 S275JR steel [49].
S275JR steel |
Chemical composition (maximum % of element) | Physical properties |
Carbon (C) | 0.210 | Density | 7.85 g/cm³ |
Manganese (Mn) | 1.500 | Melting point | 1420–1460°C |
Phosphorus (P) | 0.035 | Mechanical properties |
Sulfur (S) | 0.035 | Yield strength | 275 MPa |
Nitrogen (N) | 0.012 | Tensile strength | 410–560 MPa |
Copper (Cu) | 0.550 | Minimum percentage of elongation before fracture | 23% |
Table 2
– Shielding gas flow rate in samples.
SAMPLE | GAS FLOW (l/min.) |
01 | 12 |
02 |
03 |
04 | 15 |
05 |
06 |
07 | 20 |
08 |
09 |
The gas mixture was 75% Ar and 25% CO2. Other welding parameters remained constant, including a welding current of 186 A, voltage of 19.1 V, arc length of 10 mm, wire feed rate of 11.8 m/min, travel speed of 800 mm/min, and stick-out of 20 mm.
To perform LCR measurements with the ultrasonic devices, a flat surface is necessary to ensure proper coupling of the wedges on the samples. Consequently, a machining operation, such as milling, would be necessary on the weld bead. However, this process would modify the RS state within the material and increase the costs associated with sample preparation. For this reason, it was decided to take measurements on the opposite side from where the weld bead was deposited. This approach is feasible because the penetration depth of LCR waves is approximately one wavelength [50, 52, 53]. Using 1 MHz transducers, the LCR wave penetrates to a depth of 5.85 mm, which nearly encompasses the entire thickness of the samples (6.35 mm).
Additionally, the ultrasonic method has the advantage that the surface roughness of the material minimally affects the TOF [44]. This occurs because the LCR wave propagates just a few millimeters below the surface, depending on the frequency of the transducer. Nevertheless, it is crucial to clean the surface to remove any residues to ensure proper wedge coupling. Consequently, all samples were cleaned to eliminate dust and then hand-sanded to remove coarse imperfections and dirt. Different grades of sandpaper (80, 120, and 240) were used for this task.
Another important step is to verify the transducers to ensure accurate measurements. This verification was conducted by comparing the TOF among the three 1 MHz transducers using a standard block (steel IIW block, type 1, model SN 17-3108) and the pulse-echo method. The verification process entails applying 0.5 ml of coupling gel, attaching the transducer to the standard block, recording ten TOF values, removing the transducer, cleaning the gel, and repeating this process three times for each transducer.
The ultrasonic system for measuring RS consists of several components, each serving one or more functions to enable the measurement of the TOF of the LCR wave. Figure 3 illustrates the system divided into seven sets, and Table 3 describes the system's elements.
Table 3
– Description of the components of the ultrasonic measurement system illustrated in Fig. 3.
SET | ELEMENT | BRAND | MODEL | FUNCTION |
1 | Chassis | National Instruments | PXI-1071 | Provides a platform for hosting and interconnecting multiple PXI module |
Embedded Controller | PXIe-8840 | Controls the overall operation of the PXI system |
Oscilloscope Module | PXIe-5114 | Acquires electrical signals emitted by a transducer |
Multifunction Module | PXI-6221 | Allows the control of the electric actuator |
2 | Pulser/ Receiver | JSR Ultrasonics | DPR300 | Amplifies the signals sent and received to the emitting and receiving transducers |
3 | Temperature module | National Instruments | PXI-9213 | Enables thermocouple couplings and temperature measurement |
4 | Monitor | HP | L200hx | Transmits processed information from the computer through images |
Mouse and keyboard | Lenovo | Unknown | Inputs data into the computer |
5 | Connector Block | National Instruments | SCB-68A | Allows for signal connections |
6 | Driver | Unknown | L298N | Amplifies the electrical signal |
7 | Transducers | Technisonic | ABS-0X0408-GP | Transform electric pulses into ultrasonic waves or vice versa |
Electric actuator | Yuyao Huayi Linear Drive Technology | HY01H-12V | Applies the coupling force |
Magnetic base | Digimess | 270.240 | Allows the fixation of the device on the component to be measured |
Thermocouple | HUA LON | TP01 | Measures temperature |
The seventh component, referred to as the ultrasonic device, is designed for swift and precise adjustment of the measurement position when affixed to the samples. Apart from the elements described in Table 3, this device (set 7) features a structure comprising aluminum 6063-T5 structural profiles, connectors (corners, screws, nuts, and washers), ballscrew, bearing housings, linear guide, and acrylic wedges angled at 23.8° for transducers coupling, facilitating the generation and capture of LCR waves. Figure 4 depicts the ultrasonic device.
The time of flight of the ultrasonic wave was measured using the second zero crossing method. This method consists of detecting the first positive peak of the digitized signal from the emitting transducer in the time domain and recording the second crossing of the signal with the horizontal axis (time) after that peak as the TOF of the wave. Signal digitization was done using the PXIe-5114 oscilloscope module with an acquisition rate of 250 MS/s.
In addition, a program was created using the NI LabVIEW® graphical programming platform. This program connects with the oscilloscope board to calculate, display, and save the Time of Flight (TOF) and signal amplitude. It also connects with the external temperature module to display and save temperatures measured by thermocouples, and with the electric actuator controller (multifunction module) to enable control.
An investigation was carried out to evaluate the impact of the amount of coupling gel on TOF and signal amplitude. The objective is to identify the optimal amount of gel required for the measurements. This quantity should be minimized to reduce costs while ensuring effective coupling and transmission of LCR waves.
Three selected amounts of coupling gel were tested between the wedges and the sample: 0.25 ml, 0.5 ml, and 0.75 ml. The tests were conducted on sample 01 at the same measurement position, away from the weld bead. Initially, one of the three gel quantities was applied under each wedge. Subsequently, the coupling force was applied and TOF and signal amplitude recordings were taken every 5 seconds for 1 minute, resulting in 12 measurements. Then, the wedges are lifted, and the gel is removed. This process is repeated three times for each gel quantity, totaling 36 measurements for each amount (108 measurements overall).
The influence of coupling force was determined by measuring the time of flight (TOF) for various electric voltages supplied to the actuator. Initially, 0.5 ml of coupling gel was applied between the transducer and the wedge. Then, the voltage was supplied to the electric actuator, and ten TOF measurements were taken on sample 01 in a fixed measurement position, away from the weld bead. Subsequently, the coupling gel was cleaned. This process was repeated three times for each supplied voltage.
Temperature influence was assessed by conducting TOF measurements ranging from 18°C to 25°C and from 25°C to 18°C, with 1°C increments. Three measurements were taken at each temperature. Temperature variations were achieved using a split air conditioner. Other parameters, such as measurement position (on sample 01), coupling gel volume (0.5 ml), and coupling force (146.7 N, achieved by supplying 5.1 V to the electric actuator), were kept constant to isolate the effect of temperature on TOF.
The TOF correction was conducted using a correction factor obtained from the study of temperature influence. This factor compensates for TOF variations caused by a 1°C temperature change. The correction factor was calculated by subtracting the product of the correction factor and the difference between the measured temperature and the reference temperature (set at 20°C) from the measured TOF. Temperature was measured using three thermocouples positioned at sample 01 and the wedge connecting bar.
The RS measurement method was devised to mitigate the plate distortions arising from welding. As a result, scanning is conducted individually on each side of the weld bead. Additionally, measurements are taken from the opposite side of the weld bead deposition, eliminating the necessity for milling, thereby preserving the original RS state and reducing sample preparation costs. This method, depicted schematically in Fig. 5, enables the acquisition of the longitudinal RS distribution profile across the transverse direction to the weld bead.
The method consists of:
1) Select a sample.
2) Select one side on the bottom of the sample and fix the magnetic bases of the ultrasonic device in the position indicated in Fig. 6.
3) Move the transducers to the initial position, as shown in Fig. .
4) Apply coupling gel and coupling force.
5) Take a measurement of TOF and signal amplitude.
6) Clean the gel and move the transducers 2 mm towards the weld bead.
7) Return to step 4 until 25 measurements are taken. After 25 measurements, fix the ultrasonic device on the opposite side of the weld bead of the selected sample.
8) Complete two scans of 25 measurements on each side of the sample.
Upon completing the procedure, data processing is required. This entails converting TOF measurements into RS, correcting TOF for temperature fluctuations, and organizing the measurements of each sample to obtain the RS distribution profile.
To convert TOF into RS, Eq. 2 was used. The material's modulus of elasticity (E) was set at 210 GPa [54]. The acoustoelastic constant (L11) of 2.58 was adopted based on experimental findings from previous studies [45]. The travel time in the stress-free material (t0) was calculated by averaging the TOF readings taken at five points furthest from the weld bead on both sides of the base metal. Hence, for each sample, the stress-free material’s TOF was established by averaging the TOF readings from the ten furthest points of the weld bead. These parameters allowed the conversion of TOF (t) into stress according to Eq. 3.
$$\:\sigma\:=\frac{210.{10}^{9}}{\text{2,58}.{t}_{0}}\left(t-{t}_{0}\right)=\frac{\text{8,14}.{10}^{10}}{{t}_{0}}\left(t-{t}_{0}\right)$$
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